Crystal Structure of Poly[(2,6-di(2',4'-dicarboxylphenyl)pyridine-κ4 O:O':O":O'")-(μ2-1,4-bis(1-imidazolyl)benzene-κ2N:N')cobalt(Ⅱ)],C39H24Co2N7O8

被引：0
|
作者：
Wang Yenan [1 ]
Liu Bo [1 ]
Niu Xiaoqing [1 ]
机构：
[1] Coconut Research Institute of Chinese Academy of Tropical Agricultural Sciences, Hainan Innovation Center of Academician Team
来源：
Plant Diseases and Pests | 2021年 / 12卷 / 01期
关键词：
D O I：
10.19579/j.cnki.plant-d.p.2021.01.009
中图分类号：
O641.4 [络合物化学（配位化学）];
学科分类号：
070304 ; 081704 ;
摘要：
[Objective] The paper was to synthesize a new structure of metal organic framework,and to provide new materials for plant pathogens testing.[Method] A mixture of 2,6-di(2’,4’-di-carboxylphenyl)pyridine,1,4-bis(1-imidazolyl)benzene,Co(NO)·6HO were added to the solution of DMF:H2O=3:3 and heated at 433 K for 4 d.[Result] Red crystals of the title compound were obtained(yield 76.3%,based on Co).[Conclusion]The crystal data were obtained as follows:CHCoNO,monoclinic,P21/c,α=16.222(7) A,b=12.653(5) A,c=17.456(7) ?,β=102.386(6)°,V=3 500(2) ?~3,Z=4,Rgt(F)=0.055 0,wRref(F~2)=0.150 9,T=293(2) K.
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页码：38 / 43
页数：6
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