[Fe3O4@SiO2@Si(CH2)3-NMe2-(CH2)2-NMe2-SO3H][Cl]2 as a novel magnetic nanocatalyst for the synthesis of bis(6-amino-1,3-dimethyl-uracil-5-yl)methanes

被引:0
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作者
Zare, Abdolkarim [1 ]
Dianat, Manije [2 ]
Moosavi-Zare, Ahmad Reza [3 ,4 ]
Monfared, Fatemeh [2 ]
机构
[1] Persian Gulf Univ, Fac Nano & Bio Sci & Technol, Dept Chem, Bushehr, Iran
[2] Payame Noor Univ, Dept Chem, Tehran, Iran
[3] Shiraz Univ, Coll Sci, Chem Dept, Shiraz, Iran
[4] Hamedan Univ Technol, Dept Chem Engn, Hamadan, Iran
来源
IRANIAN JOURNAL OF CATALYSIS | 2024年 / 14卷 / 04期
关键词
Magnetic nanocatalyst; bis(6-amino-1,3- dimethyluracil-5-yl)methanes; 6-Amino-1,3-dimethyluracil; Solvent-free; ONE-POT SYNTHESIS; EFFICIENT CATALYST; IONIC LIQUID; URACIL DERIVATIVES; NANOPARTICLES; GREEN; OXIDATION; CELLULOSE; TAG;
D O I
10.57647/j.ijc.2024.1404.45
中图分类号
O64 [物理化学(理论化学)、化学物理学];
学科分类号
070304 ; 081704 ;
摘要
A new magnetic nanomaterial, namely [Fe3O4@SiO2@Si(CH2)3-NMe2-(CH2)2-NMe2-SO3H][Cl]2 (FSCNSC) was synthesized, and characterized by energy-dispersive X-ray spectroscopy (EDS), elemental mapping, field emission scanning electron microscopy (FE-SEM), X-ray diffraction (XRD), FT-IR, vibrating-sample magnetometery (VSM), thermogravimetric (TG) and derivative thermogravimetry (DTG) analyses. Afterward, it was used as a highly effective catalyst for the synthesis of bis(6-amino-1,3-dimethyluracil-5-yl)methanes under solvent-free conditions. FSCNSC was better than many of the reported catalysts for the synthesis of this category of uracil derivatives in terms of the reaction conditions, the reaction times, and yields.
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页数:14
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