This research was supported by the Division of Chemical Sciences;
Office of Basic Energy Sciences;
US Department of Energy under contract no. W-31-109-ENG-38. Work at the National Synchrotron Light Source of Brookhaven National Laboratory is supported by the US DOE under contract no. DE-AC02-76CH00016;
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ATOM ENERGY CANADA LTD,CHALK RIVER NUCL LABS,CHALK RIVER K0J 1J0,ONTARIO,CANADAATOM ENERGY CANADA LTD,CHALK RIVER NUCL LABS,CHALK RIVER K0J 1J0,ONTARIO,CANADA