Synthesis of 1,3,5-triethoxybenzene

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作者：
Hu, Yimin
Wang, Xiuran
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来源：
Jingxi Huagong/Fine Chemicals | 1998年 / 15卷 / 06期
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摘要：
The 1,3,5-(EtO)3C6Cl3 was synthesized by refluxing hexachloro-benzene C6Cl6 with NaOEt in pyridine for 3 h, then it was dechlorinated and etherified with Na in EtOH to give the 1,3,5-triethoxybenzene. The compound was identified by elementary analysis, IR and MS. The optimum conditions are as follow: a molar ratio of C6Cl6 to NaOEt is 1:6, reaction time is 3 h. The overall yield is about 61%.
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页码：31 / 33
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