RAPID: an ImageJ macro for indexing electron diffraction zone axis spot patterns of cubic materials

被引:0
|
作者
Weirich, Thomas E. [1 ]
机构
[1] Rhein Westfal TH Aachen, Gemeinschaftslabor Elekt Mikroskopie GFE, Ahornstr 55, D-52074 Aachen, Germany
来源
关键词
electron diffraction; zone axis spot patterns; Kikuchi patterns; transmission electron microscopy; orientation determination; cubic symmetry; ratio methods; ImageJ macros; RAPID; automated indexing; CRYSTALLOGRAPHIC ANALYSIS; COMPUTER-PROGRAM; SOFTWARE; TOMOGRAPHY; TOOL;
D O I
10.1107/S1600576724010215
中图分类号
O6 [化学];
学科分类号
0703 ;
摘要
As an extension to previous work, the ImageJ macro script RAPID (ratio-method pattern indexing) has been developed to allow instant indexing of calibrated and uncalibrated zone axis aligned electron diffraction patterns of cubic lattices using the R-n ratio principle. The program can be used to index zone axis aligned selected-area electron diffraction patterns, nanobeam electron diffraction patterns, transmission electron microscopy (TEM) Kikuchi patterns and even fast Fourier transforms of high-resolution (scanning) TEM images. The program allows the user to quickly assess whether the material under investigation belongs to the cubic crystal system, is pseudo-cubic or is not cubic at all by adjusting the boundary parameters and allowed errors for lattice indexing. The software also allows one to distinguish between the P, I and F Bravais lattices for certain zone axis directions. For calibrated diffraction patterns, the lattice parameters can be obtained, allowing verification of the material under investigation or phase identification in connection with a structural database. In addition, the program can be employed for determination or verification of the used instrument's camera constant when reference materials are used. Therefore, it is a convenient tool for on-site crystallographic analysis in TEM laboratories.
引用
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页码:2017 / 2029
页数:13
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