Study on Low-temperature Preparation and Hydration Properties of Calcium Sulphoaluminate-Belite Cement Clinker

被引:0
|
作者
Guo W. [1 ]
Wang C. [1 ]
Sun J. [1 ]
Chen Y. [1 ]
Yu P. [1 ]
Jiang J. [1 ]
机构
[1] School of Material Science and Engineering, Yancheng Institute of Technology, Yancheng
来源
| 1600年 / Cailiao Daobaoshe/ Materials Review卷 / 31期
关键词
Calcium sulphoaluminate-belite cement; Hydration properties; Hydrothermal synthesis; Low-temperature calcination;
D O I
10.11896/j.issn.1005-023X.2017.024.008
中图分类号
学科分类号
摘要
Coal gangue, desulfurization gypsum and lime were used as main raw materials, the calcium sulphoaluminate-belite cement clinker was prepared by hydrothermal synthesis and low-temperature calcination. The mineral phases of hydrothermal synthesis products, calcined samples and their hydration products were measured by XRD (X-ray diffraction), SEM (scanning electron microscope). The change of hydration heat of cement with time was analyzed by isothermal calorimeter, and the mechanical properties of cement were measured. The results showed that under the premise of hydrothermal synthesis of precursor at 120℃, the calcium sulphoaluminate-belite cement clinker can be completely sintered at 1 050℃. The early hydration heat release rate of this low-temperature sintered cement is higher, compared with that of one-step calcined cement. When gypsum content is 13wt% in cement, the 1 d and 28 d compressive strength of cement were 30.2 MPa and 57.3 MPa, respectively. The hydration product of cement in 28 d was mainly AFt with long fiber. © 2017, Materials Review Magazine. All right reserved.
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页码:35 / 39
页数:4
相关论文
共 14 条
  • [1] Shen Y., Qian J.S., Chai J.Q., Et al., Calcium sulphoaluminate cements made with phosphogypsum: Production issues and material properties, Cem Concr Comp, 48, (2014)
  • [2] Costa E.B., Rodriguez E.D., Bernal S.A., Et al., Production and hydration of calcium sulfoaluminate-belite cements derived from aluminium anodising sludge, Constr Build Mater, 122, (2016)
  • [3] Geng Y.J., Li S.C., Li Q.Y., Et al., Preparation of sulphoaluminate cement from petroleum coke fluidized bed combustion fly ash, Chin J Environ Eng, 10, 8, (2016)
  • [4] Zhao H.W., Li J.H., Liu H., Hydrated properties and mineralogical composition of sulphoaluminate cement clinker made from red mud, Nonferrous Metal, 58, 4, (2006)
  • [5] Shi H.S., Wu K., Guo X.L., Et al., Preparation of sulphoaluminate cement from municipal solid waste incineration fly ash and its hydration properties, J Build Mater, 14, 6, (2011)
  • [6] Adolfsson D., Menad N., Viggh E., Et al., Steelmaking slags as raw material for sulphoaluminate belite cement, Adv Cem Res, 19, 4, (2007)
  • [7] Yang N.R., Zhong B.Q., A study on active β-dicalcium silicate, J Chin Ceram Soc, 10, 2, (1982)
  • [8] Gong Y.F., Fang Y.H., Preparation of belite cement from stockpiled high-carbon fly ash using granule-hydrothermal synthesis method, Constr Build Mater, 111, (2016)
  • [9] Rungchet A., Chindaprasirt P., Wansom S., Et al., Hydrothermal synthesis of calcium sulfoaluminate-belite cement from industrial waste materials, J Clean Prod, 115, (2016)
  • [10] Guo W., Li D.X., Chen J.H., Et al., Early hydration process of cement with mechanically activated burned coal gangue, J Chin Ceram Soc, 36, 1, (2008)