Optimization research of base-phosphogypsum cemented backfill ratio based on orthogonal test

被引:4
|
作者
Zhao F.-W. [1 ]
Hu J.-H. [1 ]
Zeng P.-P. [1 ]
Wang X.-L. [2 ]
Zhao L. [2 ]
机构
[1] School of Resources and Safety Engineering, Central South University, Changsha
[2] Hubei Sanning Mining Co., Ltd., Yichang
基金
中国国家自然科学基金;
关键词
Index value prediction method; Matrix analysis method; Orthogonal test; Range method; Relationship model;
D O I
10.11817/j.ysxb.1004.0609.2021-37729
中图分类号
学科分类号
摘要
The filling technology of phosphogypsum as aggregate is one of the treatment methods of goaf and solid waste, and phosphogypsum's chemical activity is the key to affect the filling effect. Taking phosphogypsum filling to be carried out in a mine as the object,and the base in quicklime was used as an activator. According to the orthogonal experiment method, 16 groups of ratios were designed to carry out combined experiments. The range method was used to analyze the optimal ratio under each index (slump, 3 d compressive strength, 7 d compressive strength and 28 d compressive strength), and the matrix analysis method was used to analysis and optimize to obtain the feasible optimal ratio, and the index value prediction method was used to predict the mechanical characteristic value of the final ratio. The results indicate that: 1) The content of phosphogypsum is the first main influencing factor under various indexes, and the second main influencing factors for the three indexes of slump, 3 d strength and 7 d strength next time are the slurry concentration. Under the 28 d strength index, the second main influencing factor is lime content. 2) The final parameters of the optimally selected backfill are as follows: phosphogypsum of 20%, cement to tailings ratio of 1:6, slurry concentration of 80%, and quicklime of 1%. Its estimated values of mechanical properties are slump of 10.1936 cm, 3 d strength of 0.6108 MPa, 7 d strength of 1.2734 MPa, 28 d strength of 2.5748 MPa. 3) The influence relation model of different factors is established. The relationship between various index values (slump, 3 d strength and 7 d strength) and the main influencing factors are in accordance with the relationship of Z=Ax2+By2+Cx+Dy+Exy+F. © 2021, Science Press. All right reserved.
引用
收藏
页码:1096 / 1105
页数:9
相关论文
共 15 条
  • [1] LIUY K, ZHANGQ L, CHEN Q S, Et al., Utilisation of water-washing pre-treated phosphogypsum for cemented paste backfill, Minerals, 9, 3, pp. 1-19, (2019)
  • [2] ZHANG Zheng, YANG Zhi-qiang, GAO Qian, Experiment of filling cementitious material formula based on Phosphogypsum with high early-age strength in Jinchuan Mine, Industrial Minerals and Processing, 1, pp. 31-35, (2016)
  • [3] XIAO Bo-lin, YANG Zhi-qiang, GAO Qian, Development of new filling cementitious material of phosphogypsum in Jinchuan Mine, Mining Research and Development, 35, 1, pp. 21-24, (2015)
  • [4] ZHANG Guang-cun, YANG Zhi-qiang, GAO Qian, Et al., Development of early strength filling cementing material with phosphogypsum as substitute of traditional cement, Metal Mine, 3, pp. 194-198, (2015)
  • [5] YANG Xiao, Development of phosphogypsum-based early-strength cementitious material and resources utilization of waste, (2016)
  • [6] WU Shi-long, LU Ting-hao, YANG De-xi, Study on engineering properties of limed phosphogypsum by indoor tests, Jiangsu Architecture, 6, pp. 49-51, (2007)
  • [7] HU Jian-hua, XUE Xiao-meng, LEI Tao, Et al., Orthogonal experiments on impact break of induction caving to caking ore, Journal of Central South University(Science and Technology), 12, pp. 5032-5037, (2013)
  • [8] WANG Xin-min, HU Yi-bo, WANG Shi, Et al., Orthogonal test of optimization of ultrafine whole-tailings backfill materials, Gold Science and Technology, 23, 3, pp. 45-49, (2015)
  • [9] LIX B, ZHOUY A, ZHU Q Q, Et al., slurry preparation effects on the cemented phosphogypsum backfill through an orthogonal experiment, Minerals, 9, 1, pp. 1-18, (2019)
  • [10] LI Di-yuan, SUN Cheng-zhi, JIAN Ming-xing, Et al., Strength characteristics of cemented backfilling with phosphogypsum and mullock based on orthogonal experiment, Chinese Journal of Underground Space and Engineering, 13, 1, pp. 29-34, (2017)