Bis(4-benzoyl-3-methyl-1-phenyl-4,5-dihydro-1H-pyrazol-5-olato-kappa O-2,O ')-(methanol-kappa O)dioxidouranium(VI) methanol monosolvate

被引：0

作者：

Dehbi, Ouarda ^{[1
]}

Keraghel, Saida ^{[1
]}

Bouacida, Sofiane ^{[2
]}

Benghanem, Fatiha ^{[1
]}

Ourari, Ali ^{[1
]}

机构：

[1] Univ Farhat Abbas, Fac Sci Ingn, LEIMCR, Setif 19000, Algeria

[2] Univ Mentouri Constantine, CHEMS, Unite Rech Chim Environnement & Mole Struct, Setif 25000, Algeria

来源：

ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS | 2012年 / 68卷

关键词：

D O I：

10.1107/S1600536812011075

中图分类号：

O7 [晶体学];

学科分类号：

0702 ; 070205 ; 0703 ; 080501 ;

摘要：

In the title compound, [U(C17H13N2O2)(2)O-2(CH3OH)]center dot CH3OH, the U-VI ion is coordinated by seven O atoms in a distorted pentagonal-bipyramidal geometry with two 3-methyl-1-phenyl-4-benzoyl-4,5-dihydro-1H-pyrazol-5-olate groups with two O atoms in a bidentate chelating coordination mode and by three O atoms, one of which is from a methanol ligand. The crystal packing can be described by alternating layers of complex molecules along the a axis. The structure is stabilized by O-H center dot center dot center dot N and O-H center dot center dot center dot O hydrogen bonding and van der Waals interactions.

引用

页码：M457 / +

页数：12

共 50 条

[1] Bis(4-benzoyl-3-methyl-1-phenyl-1H-pyrazol-5-olato- kappa(2) O,O ')bis(ethanol-kappa O)-cobalt(II)
Idemudia, Omoruyi G.
Hosten, Eric C.
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : M1107 - +
[2] (Methanol-kappa O){1-[ 2-(piperazin-4-ium-1yl-kappa N-1)ethyliminomethyl-kappa N]naphthalen-2-olato-kappa O} bis(thiocyanato-kappa N)-nickel(II) methanol monosolvate
Li, Pin-Ai
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : M549 - +
[3] Tetrakis(mu-2-phenylquinoline-4-carboxylato-kappa O-2: O ')bis[(methanol-kappa O)copper(II)]
Guo, Junfang
Yan, Guoping
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : M1296 - +
[4] Crystal structure of [bis(2,6-diisopropylphenyl) phosphato-kappa O]tris(methanol-kappa O)lithium methanol monosolvate
Minyacy, Mikhail F.
Nifant'ev, Ilya F.
Taytorkin, Alexander N.
Korchagina, Sof'ya A.
Zeynalova, Shadana Sh
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2015, 71 : 443 - +
[5] (mu-Acetato-kappa O-2:O')[mu-2,6-bis({bis[(pyridin-2-yl-kappa N)methyl]amino-kappa N}methyl)-4-methylphenolato-kappa O-2:O](methanol-kappa O)dizinc bis(perchlorate)
Das, Biswanath
Haukka, Matti
Nordlander, Ebbe
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2014, 70 : M120 - +
[6] Bis[4-(4-chlorobenzoyl)-3-methyl-1-phenyl-1H-pyrazol-5-olato-κ2O,O′]bis(methanol-κO)nickel(II)
Zhang, Xin
Huang, Meng
Du, Cong
Han, Junjing
ACTA CRYSTALLOGRAPHICA SECTION E-STRUCTURE REPORTS ONLINE, 2010, 66 : M1361 - U252
[7] Bis(4,4''-difluoro-1,1':3',1''-terphenyl-2'carboxylato- kappa O) tetrakis( methanol-kappa O)calcium methanol tetrasolvate
Kim, Namseok
Noh, Heeso
Yoon, Sungho
Park, Chan Ryang
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2013, 69 : M122 - +
[8] Crystal structure of bis(4-benzoyl-3-methyl-1-phenyl-4,5-dihydro-1H-pyrazol-5-onato)-(ethanol)-dioxourane(VI) ethanol solvate
Chumakov, Yu. M.
Petrenko, P. A.
Julea, F. G.
Tsapkov, V. I.
Gulea, A. P.
JOURNAL OF STRUCTURAL CHEMISTRY, 2014, 55 (06) : 1116 - 1119
[9] Crystal structure of bis(4-benzoyl-3-methyl-1-phenyl-4,5-dihydro-1H-pyrazol-5-onato)-(ethanol)-dioxourane(VI) ethanol solvate
Yu. M. Chumakov
P. A. Petrenko
F. G. Julea
V. I. Tsapkov
A. P. Gulea
Journal of Structural Chemistry, 2014, 55 : 1116 - 1119
[10] Bis(1,2-dimethoxyethane)-1 kappa O-2,O ';3 kappa O-2,O '-tetrakis(mu-1,1,1,3,3,3-hexafluoro-2-methylpropan-2-olato)1: 2 kappa(4) O:O;2: 3 kappa(4) O:O-1,3-dilithium-2magnesium
Wurst, Klaus
Buchmeiser, Michael R.
ACTA CRYSTALLOGRAPHICA SECTION E-CRYSTALLOGRAPHIC COMMUNICATIONS, 2012, 68 : M1106 - +

← 1 2 3 4 5 →