SYNTHESIS, SEPARATION AND CHARACTERIZATION OF UNSYMMETRICALLY SUBSTITUTED PHTHALOCYANINES

被引：56
|
作者：
LINSSEN, TG [1 ]
HANACK, M [1 ]
机构：
[1] UNIV TUBINGEN,INST ORGAN CHEM,LEHRSTUHL ORGAN CHEM 2,MORGENSTELLE 18,D-72076 TUBINGEN,GERMANY
来源：
CHEMISCHE BERICHTE | 1994年 / 127卷 / 10期
关键词：
PHTHALOCYANINES; UNSYMMETRICALLY SUBSTITUTED; CHROMATOGRAPHIC SEPARATION;
D O I：
10.1002/cber.19941271030
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
Unsymmetrically substitued (phthalocyaninato)nickel(II) complexes 3-7 were synthesized by statistical condensation of 4,5-dipentoxy- (2a), 4,5-diheptyl- (2b), 3,6-dihexoxy- (2c), and 3,6-diheptylphthalonitrile (2d) with 3,4,5,6-tetraphenylphthalonitrile (1) and separated by column chromatography. The obtained phthalocyanines 3-7 were characterized by UV-, IR-, and H-1-NMR spectroscopy.
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页码：2051 / 2057
页数：7
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