SIMULTANEOUS MICRODETERMINATION OF CARBON, HYDROGEN AND LEAD IN ORGANOLEAD COMPOUNDS

被引:1
|
作者
HASSAN, HNA
HASSOUNA, MEM
GAWARGIOUS, YA
机构
[1] Microanalytical Research Laboratory, National Research Centre, Dokki, Cairo
[2] Faculty of Science at Beni-Suef, Cairo University
关键词
MICROANALYSIS; SIMULTANEOUS C-DETERMINATION; H-DETERMINATION; PB-DETERMINATION AND S-DETERMINATION;
D O I
10.1007/BF01772351
中图分类号
O65 [分析化学];
学科分类号
070302 ; 081704 ;
摘要
The straight emtpy-tube method of Korshun and Klimova has been successfully extended to the simultaneous microdetermination of carbon, hydrogen and lead in organolead compounds. In all cases, the lead content was calculated from the weight of the plumbous oxide residue left behind in the fused-silica capsule used to hold the sample. Sulphur could also be determined in the same analysis. Satisfactory results were obtained for all compounds with a standard deviation not exceeding 0.1%.
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页码:37 / 40
页数:4
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