PREPARATION AND CHARACTERIZATION OF SIO2-SB2O3 FILMS OBTAINED BY A SOL-GEL METHOD

被引:1
|
作者
PARLOG, C
GARTNER, M
VASILESCU, A
DRAGAN, N
机构
[1] Institute of Physical Chemistry, Bucharest, 77208
关键词
D O I
10.1016/0022-3093(92)90016-D
中图分类号
TQ174 [陶瓷工业]; TB3 [工程材料学];
学科分类号
0805 ; 080502 ;
摘要
SiO2-Sb2O3 films 600-800 angstrom thick were spin-coated on polycrystalline silicon from a sol prepared from tetraethylorthosilicate and antimony trichloride. One hour heat treatment at 500, 1000 and 1150-degrees-C resulted in crack-free, vitreous, homogeneous films in the first two cases, while at 1200-degrees-C crystallization started to occur. The thickness and refractive index of the films were dependent on the heat treatment. Optical and structural properties of the films were characterized by X-ray, IR spectroscopy, ellipsometry, absorption spectroscopy and electron microscopy. UV absorption spectrum of the SiO2-Sb2O3 films shows discernable bands of pure Sb2O3.
引用
收藏
页码:109 / 114
页数:6
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