ADDUCT OF 2 1,8-NAPHTHYRIDINE MOLECULES (ONE PROTONATED) WITH TETRACHLOROFERRATE(III)

被引：13
|
作者：
BARBARO, P
BIANCHINI, C
FOCHI, M
MASI, D
MEALLI, C
机构：
[1] Istituo per lo Studio della Stereochimica ed Energetica dei Composti di Coordinazione, CNR, Via J. Nardi 39, Firenze
来源：
ACTA CRYSTALLOGRAPHICA SECTION C-CRYSTAL STRUCTURE COMMUNICATIONS | 1992年 / 48卷
关键词：
D O I：
10.1107/S0108270191011149
中图分类号：
O6 [化学];
学科分类号：
0703 ;
摘要：
1,8-Naphthyridinium tetrachloroferrate(III)-1,8-naphthyridine (1/1), C8H7N2+.FeCl4-.-C8H6N2, M(r) = 458.9, monoclinic, Cc, a = 10.698 (2), b = 25.533 (4), c = 7.315 (2) angstrom, beta = 101.83 (1)-degrees, V = 1955.67 (72) angstrom 3, Z = 4, D(x) = 1.5588 Mg m-3, lambda(Cu K-alpha) = 1.5418 angstrom, mu = 11.4 mm-1, F(000) = 924, room temperature, final R = 0.0704 for 929 reflections. The structure consists of discrete tetrahedral FeCl4- anions, protonated (NNH)+ and unprotonated (NN) 1,8-naphthyridine molecules.
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页码：625 / 627
页数：3
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