The amazing effects and role of PVP on the crystallinity, phase composition and morphology of nickel ferrite nanoparticles prepared by thermal treatment method

被引：0
|
作者：
Naseri, Mahmoud Goodarz [1 ,2 ]
Saion, Elias [2 ]
Zadeh, Nasrin Khalil [2 ]
机构：
[1] Malayer Univ, Fac Sci, Dept Phys, Arak St, Malayer 6571995863, Iran
[2] Univ Putra Malaysia, Fac Sci, Dept Phys, Serdang 43400, Selangor, Malaysia
来源：
INTERNATIONAL NANO LETTERS | 2013年 / 3卷 / 01期
关键词：
Nanostructures; X-ray diffraction; Infrared spectroscopy; Magnetic properties;
D O I：
10.1186/2228-5326-3-19
中图分类号：
TB3 [工程材料学];
学科分类号：
0805 ; 080502 ;
摘要：
Nickel ferrite nanocrystals were prepared from an aqueous solution containing metal nitrates and various concentrations of poly(vinylpyrrolidone) followed by calcination temperature. X-ray diffraction (XRD) analysis was performed to determine the degree of crystallinity of the ferrite nanoparticles. By transmission electron microscopy, the morphology and average particle size of the nickel ferrite nanoparticles were evaluated which had good agreement with the XRD results. Fourier transform infrared spectroscopy suggested the presence of metal oxide bands in all samples as well as the effective elimination of organic constituents after calcinations. Measurements of the extent of magnetization of the nickel ferrite nanoparticles synthesized in different concentrations were obtained at room temperature using a vibrating sample magnetometer.
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页数：8
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