SAMPLE PREPARATION PROCEDURE FOR THE DETERMINATION OF SULFUR AND TRACE-METALS IN OIL PRODUCTS BY THE ICP WITH A MINITORCH USING EMULSIONS

被引：22
|
作者：
BORSZEKI, J
KNAPP, G
HALMOS, P
BARTHA, L
机构：
[1] GRAZ UNIV TECHNOL,INST ANALYT CHEM MICRO & RADIOCHEM,A-8010 GRAZ,AUSTRIA
[2] UNIV VESZPREM,DEPT MINERAL OIL & COAL TECHNOL,H-8201 VESZPREM,HUNGARY
[3] HUNGARY ACAD SCI,DEPT ANALYT CHEM,RES GRP,H-8201 VESZPREM,HUNGARY
来源：
MIKROCHIMICA ACTA | 1992年 / 108卷 / 3-6期
关键词：
SULFUR; TRACE METALS; EMULSIONS; INDUCTIVELY COUPLED PLASMA SPECTROMETRY; OIL;
D O I：
10.1007/BF01242425
中图分类号：
O65 [分析化学];
学科分类号：
070302 ; 081704 ;
摘要：
A quick sample preparation method was used for the determination of sulphur and trace metals in oil and oily products by the ICP with a minitorch. Stable aqueous emulsions of oils and oil products were made by using two kinds of emulsifiers (one with low sulphur content, the other sulfonated). Aqueous standard solutions can be used for the preparation of calibration solutions. The contents of S, Al, Cr, Cu, Fe, Mg, Ni and Pb in aqueous emulsions were determined and the results were in good agreement with the composition of oil standard solutions used for control analysis procedure.
引用
收藏
页码：157 / 161
页数：5
相关论文
共 50 条
  • [1] Sample preparation in the determination of metals in oil and petroleum products by ICP MS
    A. V. Soin
    T. A. Maryutina
    T. V. Arbuzova
    B. Ya. Spivakov
    Journal of Analytical Chemistry, 2010, 65 : 571 - 576
  • [2] Sample preparation in the determination of metals in oil and petroleum products by ICP MS
    Soin, A. V.
    Maryutina, T. A.
    Arbuzova, T. V.
    Spivakov, B. Ya.
    JOURNAL OF ANALYTICAL CHEMISTRY, 2010, 65 (06) : 571 - 576
  • [3] A NOVEL SAMPLE PREPARATION TECHNIQUE FOR THE DETERMINATION OF SULFUR IN OIL PRODUCTS BY THE ICP-OES METHOD
    BORSZEKI, J
    BARTHA, L
    ACTA CHIMICA HUNGARICA-MODELS IN CHEMISTRY, 1991, 128 (4-5): : 633 - 637
  • [4] DETERMINATION OF TRACE-METALS IN HYDROTHERMAL CALCITES BY ICP-METHODS
    LUCK, JH
    LUDERS, V
    MIKROCHIMICA ACTA, 1989, 3 (3-6) : 329 - 336
  • [5] DETERMINATION OF TRACE-METALS IN COTTONSEED OIL AND HYDROGENATED COTTONSEED OIL
    ABDELRAHMAN, AHY
    FOOD CHEMISTRY, 1984, 13 (02) : 161 - 163
  • [6] USING FORAGING HONEYBEES TO SAMPLE AN AREA FOR TRACE-METALS
    FREE, JB
    WILLIAMS, IH
    PINSENT, RJFH
    TOWNSHEND, A
    BASI, MS
    GRAHAM, CL
    ENVIRONMENT INTERNATIONAL, 1983, 9 (01) : 9 - 12
  • [7] DETERMINATION OF TRACE-METALS IN SOIL SAMPLES AND PLANT-TISSUES USING ICP-OES
    KANICKY, V
    TOMAN, J
    POVOLNY, A
    KOPICOVA, Z
    CHEMICKE LISTY, 1989, 83 (02): : 194 - 204
  • [8] SIMULTANEOUS DETERMINATION OF TRACE-METALS IN SAUDI ARABIAN CRUDE-OIL PRODUCTS BY INDUCTIVELY COUPLED PLASMA MASS-SPECTROMETRY (ICP MS)
    ALSWAIDAN, HM
    ANALYTICAL LETTERS, 1988, 21 (08) : 1487 - 1497
  • [9] APPLICATION OF A SIMPLE PROCEDURE OF DIGESTION FOR THE DETERMINATION OF TRACE-METALS IN MARINE ORGANISMS
    HERNANDEZ, FH
    MEDINA, J
    ANSUATEGUI, J
    LOPEZ, FJ
    ANALUSIS, 1990, 18 (05) : 327 - 330
  • [10] ANALYSIS OF PETROLEUM FOR TRACE-METALS - DETERMINATION OF MERCURY IN PETROLEUM AND PETROLEUM-PRODUCTS
    KNAUER, HE
    MILLIMAN, GE
    ANALYTICAL CHEMISTRY, 1975, 47 (08) : 1263 - 1268
12345